Abstract

We synthesized anisotropic Pd nanoplates for use as a novel refractive index (RI) sensing material in the visible region. The nanoplates showed an extinction peak that was attributed to the excitation of the localized surface plasmon resonance at ~620 nm in the visible region. It was found that the peak was red-shifted with increasing the RI of the surrounding medium. The susceptibility was calculated to be 250 nm per RI unit, comparable to some anisotropic Au nanoparticles that are excellent RI sensing materials.

© 2016 Optical Society of America

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References

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  5. M. Thämer, A. Kartouzian, P. Heister, T. Lünskens, S. Gerlach, and U. Heiz, “Small supported plasmonic silver clusters,” Small 10(12), 2340–2344 (2014).
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    [Crossref] [PubMed]
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    [Crossref] [PubMed]
  24. N. Omura, I. Uechi, and S. Yamada, “Comparison of plasmonic sensing between polymer- and silica-coated gold nanorods,” Anal. Sci. 25(2), 255–259 (2009).
    [Crossref] [PubMed]
  25. P. K. Jain, X. Huang, I. H. El-Sayed, and M. A. El-Sayed, “Noble metals on the nanoscale: optical and photothermal properties and some applications in imaging, sensing, biology, and medicine,” Acc. Chem. Res. 41(12), 1578–1586 (2008).
    [Crossref] [PubMed]
  26. C. L. Nehl, H. Liao, and J. H. Hafner, “Optical properties of star-shaped gold nanoparticles,” Nano Lett. 6(4), 683–688 (2006).
    [Crossref] [PubMed]
  27. J. Lee, W. Hasan, and T. W. Odom, “Tuning the thickness and orientation of single Au pyramids for improved refractive index sensitivities,” J Phys Chem C Nanomater Interfaces 113(6), 2205–2207 (2009).
    [Crossref] [PubMed]
  28. Y. Khalavka, J. Becker, and C. Sönnichsen, “Synthesis of rod-shaped gold nanorattles with improved plasmon sensitivity and catalytic activity,” J. Am. Chem. Soc. 131(5), 1871–1875 (2009).
    [Crossref] [PubMed]
  29. M. J. Banholzer, N. Harris, J. E. Millstone, G. C. Schatz, and C. A. Mirkin, “abnormally large plasmonic shifts in silica-protected gold triangular nanoprisms,” J. Phys. Chem. C 114(16), 7521–7526 (2010).
    [Crossref]
  30. D. E. Charles, D. Aherne, M. Gara, D. M. Ledwith, Y. K. Gun’ko, J. M. Kelly, W. J. Blau, and M. E. Brennan-Fournet, “Versatile solution phase triangular silver nanoplates for highly sensitive plasmon resonance sensing,” ACS Nano 4(1), 55–64 (2010).
    [Crossref] [PubMed]
  31. A. J. Haes and R. P. Van Duyne, “A Nanoscale Optical Biosensor: Sensitivity and selectivity of an approach based on the localized surface plasmon resonance spectroscopy of triangular silver nanoparticles,” J. Am. Chem. Soc. 124(35), 10596–10604 (2002).
    [Crossref] [PubMed]
  32. K. Sugawa, D. Tanaka, T. Ichikawa, and N. Takeshima, “Development of plasmon resonance sensing based on alkylthiol-coated triangular silver nanoplates on glass plates,” Jpn. J. Appl. Phys. 52(4), 04CK06 (2013).
    [Crossref]
  33. L. J. Sherry, S.-H. Chang, G. C. Schatz, R. P. Van Duyne, B. J. Wiley, and Y. Xia, “Localized surface plasmon resonance spectroscopy of single silver nanocubes,” Nano Lett. 5(10), 2034–2038 (2005).
    [Crossref] [PubMed]
  34. M. A. Mahmoud and M. A. El-Sayed, “Gold nanoframes: very high surface plasmon fields and excellent near-infrared sensors,” J. Am. Chem. Soc. 132(36), 12704–12710 (2010).
    [Crossref] [PubMed]
  35. E. M. Larsson, J. Alegret, M. Käll, and D. S. Sutherland, “Sensing characteristics of NIR localized surface plasmon resonances in gold nanorings for application as ultrasensitive biosensors,” Nano Lett. 7(5), 1256–1263 (2007).
    [Crossref] [PubMed]
  36. K. Sugawa, H. Tahara, A. Yamashita, J. Otsuki, T. Sagara, T. Harumoto, and S. Yanagida, “Refractive index susceptibility of the plasmonic palladium nanoparticle: potential as the third plasmonic sensing material,” ACS Nano 9(2), 1895–1904 (2015).
    [Crossref] [PubMed]
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    [Crossref] [PubMed]
  39. K. Sugasawa, “Regulation of damage recognition in mammalian global genomic nucleotide excision repair,” Mutat. Res. 685(1-2), 29–37 (2010).
    [Crossref] [PubMed]
  40. X. Huang, S. Tang, X. Mu, Y. Dai, G. Chen, Z. Zhou, F. Ruan, Z. Yang, and N. Zheng, “Freestanding palladium nanosheets with plasmonic and catalytic properties,” Nat. Nanotechnol. 6(1), 28–32 (2011).
    [Crossref] [PubMed]
  41. J. Waxenegger, A. Trügler, and U. Hohenester, “Plasmonics simulations with the MNPBEM toolbox: Consideration of substrates and layer structures,” Comput. Phys. Commun. 193, 138–150 (2015).
    [Crossref]
  42. T. Pakizeh, C. Langhammer, I. Zorić, P. Apell, and M. Käll, “Intrinsic Fano Interference of Localized Plasmons in Pd Nanoparticles,” Nano Lett. 9(2), 882–886 (2009).
    [Crossref] [PubMed]
  43. T. A. F. König, P. A. Ledin, J. Kerszulis, M. A. Mahmoud, M. A. El-Sayed, J. R. Reynolds, and V. V. Tsukruk, “Electrically tunable plasmonic behavior of nanocube-polymer nanomaterials induced by a redox-active electrochromic polymer,” ACS Nano 8(6), 6182–6192 (2014).
    [Crossref] [PubMed]
  44. C. Langhammer, Z. Yuan, I. Zorić, and B. Kasemo, “Plasmonic properties of supported Pt and Pd nanostructures,” Nano Lett. 6(4), 833–838 (2006).
    [Crossref] [PubMed]
  45. A. S. Alkindi, Y. M. Al-Wahaibi, and A. H. Muggeridge, “Physical properties (density, excess molar volume, viscosity, surface tension, and refractive index) of ethanol + glycerol,” J. Chem. Eng. Data 53(12), 2793–2796 (2008).
    [Crossref]
  46. Y. H. Lee, H. Chen, Q.-H. Xu, and J. Wang, “Refractive index sensitivities of noble metal nanocrystals: the effects of multipolar plasmon resonances and the metal type,” J. Phys. Chem. C 115(16), 7997–8004 (2011).
    [Crossref]
  47. J. McPhillips, A. Murphy, M. P. Jonsson, W. R. Hendren, R. Atkinson, F. Höök, A. V. Zayats, and R. J. Pollard, “High-performance biosensing using arrays of plasmonic nanotubes,” ACS Nano 4(4), 2210–2216 (2010).
    [Crossref] [PubMed]

2015 (4)

T. Lünskens, P. Heister, M. Thämer, C. A. Walenta, A. Kartouzian, and U. Heiz, “Plasmons in supported size-selected silver nanoclusters,” Phys. Chem. Chem. Phys. 17(27), 17541–17544 (2015).
[Crossref] [PubMed]

K. Sugawa, H. Tahara, A. Yamashita, J. Otsuki, T. Sagara, T. Harumoto, and S. Yanagida, “Refractive index susceptibility of the plasmonic palladium nanoparticle: potential as the third plasmonic sensing material,” ACS Nano 9(2), 1895–1904 (2015).
[Crossref] [PubMed]

A. M. Pisoschi and A. Pop, “The role of antioxidants in the chemistry of oxidative stress: A review,” Eur. J. Med. Chem. 97(5), 55–74 (2015).
[Crossref] [PubMed]

J. Waxenegger, A. Trügler, and U. Hohenester, “Plasmonics simulations with the MNPBEM toolbox: Consideration of substrates and layer structures,” Comput. Phys. Commun. 193, 138–150 (2015).
[Crossref]

2014 (5)

T. A. F. König, P. A. Ledin, J. Kerszulis, M. A. Mahmoud, M. A. El-Sayed, J. R. Reynolds, and V. V. Tsukruk, “Electrically tunable plasmonic behavior of nanocube-polymer nanomaterials induced by a redox-active electrochromic polymer,” ACS Nano 8(6), 6182–6192 (2014).
[Crossref] [PubMed]

J. Cadet and J. R. Wagner, “Oxidatively generated base damage to cellular DNA by hydroxyl radical and one-electron oxidants: similarities and differences,” Arch. Biochem. Biophys. 557(1), 47–54 (2014).
[Crossref] [PubMed]

Y. Yang, I. I. Kravchenko, D. P. Briggs, and J. Valentine, “All-dielectric metasurface analogue of electromagnetically induced transparency,” Nat. Commun. 5, 5753 (2014).
[Crossref] [PubMed]

M. Thämer, A. Kartouzian, P. Heister, T. Lünskens, S. Gerlach, and U. Heiz, “Small supported plasmonic silver clusters,” Small 10(12), 2340–2344 (2014).
[Crossref] [PubMed]

G. M. Akselrod, C. Argyropoulos, T. B. Hoang, C. Ciracì, C. Fang, J. Huang, D. R. Smith, and M. H. Mikkelsen, “Probing the mechanisms of large Purcell enhancement in plasmonic nanoantennas,” Nat. Photonics 8(11), 835–840 (2014).
[Crossref]

2013 (2)

S. Campione, S. M. Adams, R. Ragan, and F. Capolino, “Comparison of electric field enhancements: linear and triangular oligomers versus hexagonal arrays of plasmonic nanospheres,” Opt. Express 21(7), 7957–7973 (2013).
[Crossref] [PubMed]

K. Sugawa, D. Tanaka, T. Ichikawa, and N. Takeshima, “Development of plasmon resonance sensing based on alkylthiol-coated triangular silver nanoplates on glass plates,” Jpn. J. Appl. Phys. 52(4), 04CK06 (2013).
[Crossref]

2012 (3)

L. Tian, J. J. Morrissey, R. Kattumenu, N. Gandra, E. D. Kharasch, and S. Singamaneni, “Bioplasmonic paper as a platform for detection of kidney cancer biomarkers,” Anal. Chem. 84(22), 9928–9934 (2012).
[Crossref] [PubMed]

P. L. Truong, B. W. Kim, and S. J. Sim, “Rational aspect ratio and suitable antibody coverage of gold nanorod for ultra-sensitive detection of a cancer biomarker,” Lab Chip 12(6), 1102–1109 (2012).
[Crossref] [PubMed]

S. M. Adams, S. Campione, J. D. Caldwell, F. J. Bezares, J. C. Culbertson, F. Capolino, and R. Ragan, “Non-lithographic SERS substrates: tailoring surface chemistry for Au nanoparticle cluster assembly,” Small 8(14), 2239–2249 (2012).
[Crossref] [PubMed]

2011 (6)

J. J. Mock, S. M. Norton, S.-Y. Chen, A. A. Lazarides, and D. R. Smith, “Electromagnetic Enhancement Effect Caused by Aggregation on SERS-Active Gold Nanoparticles,” Plasmonics 6(1), 113–124 (2011).
[Crossref]

V. Giannini, A. I. Fernández-Domínguez, S. C. Heck, and S. A. Maier, “Plasmonic nanoantennas: fundamentals and their use in controlling the radiative properties of nanoemitters,” Chem. Rev. 111(6), 3888–3912 (2011).
[Crossref] [PubMed]

Y.-F. Chang, S.-H. Hung, Y.-J. Lee, R.-C. Chen, L.-C. Su, C.-S. Lai, and C. Chou, “Discrimination of breast cancer by measuring prostate-specific antigen levels in women’s serum,” Anal. Chem. 83(13), 5324–5328 (2011).
[Crossref] [PubMed]

K. M. Mayer and J. H. Hafner, “Localized surface plasmon resonance sensors,” Chem. Rev. 111(6), 3828–3857 (2011).
[Crossref] [PubMed]

X. Huang, S. Tang, X. Mu, Y. Dai, G. Chen, Z. Zhou, F. Ruan, Z. Yang, and N. Zheng, “Freestanding palladium nanosheets with plasmonic and catalytic properties,” Nat. Nanotechnol. 6(1), 28–32 (2011).
[Crossref] [PubMed]

Y. H. Lee, H. Chen, Q.-H. Xu, and J. Wang, “Refractive index sensitivities of noble metal nanocrystals: the effects of multipolar plasmon resonances and the metal type,” J. Phys. Chem. C 115(16), 7997–8004 (2011).
[Crossref]

2010 (5)

J. McPhillips, A. Murphy, M. P. Jonsson, W. R. Hendren, R. Atkinson, F. Höök, A. V. Zayats, and R. J. Pollard, “High-performance biosensing using arrays of plasmonic nanotubes,” ACS Nano 4(4), 2210–2216 (2010).
[Crossref] [PubMed]

K. Sugasawa, “Regulation of damage recognition in mammalian global genomic nucleotide excision repair,” Mutat. Res. 685(1-2), 29–37 (2010).
[Crossref] [PubMed]

M. J. Banholzer, N. Harris, J. E. Millstone, G. C. Schatz, and C. A. Mirkin, “abnormally large plasmonic shifts in silica-protected gold triangular nanoprisms,” J. Phys. Chem. C 114(16), 7521–7526 (2010).
[Crossref]

D. E. Charles, D. Aherne, M. Gara, D. M. Ledwith, Y. K. Gun’ko, J. M. Kelly, W. J. Blau, and M. E. Brennan-Fournet, “Versatile solution phase triangular silver nanoplates for highly sensitive plasmon resonance sensing,” ACS Nano 4(1), 55–64 (2010).
[Crossref] [PubMed]

M. A. Mahmoud and M. A. El-Sayed, “Gold nanoframes: very high surface plasmon fields and excellent near-infrared sensors,” J. Am. Chem. Soc. 132(36), 12704–12710 (2010).
[Crossref] [PubMed]

2009 (4)

N. Omura, I. Uechi, and S. Yamada, “Comparison of plasmonic sensing between polymer- and silica-coated gold nanorods,” Anal. Sci. 25(2), 255–259 (2009).
[Crossref] [PubMed]

J. Lee, W. Hasan, and T. W. Odom, “Tuning the thickness and orientation of single Au pyramids for improved refractive index sensitivities,” J Phys Chem C Nanomater Interfaces 113(6), 2205–2207 (2009).
[Crossref] [PubMed]

Y. Khalavka, J. Becker, and C. Sönnichsen, “Synthesis of rod-shaped gold nanorattles with improved plasmon sensitivity and catalytic activity,” J. Am. Chem. Soc. 131(5), 1871–1875 (2009).
[Crossref] [PubMed]

T. Pakizeh, C. Langhammer, I. Zorić, P. Apell, and M. Käll, “Intrinsic Fano Interference of Localized Plasmons in Pd Nanoparticles,” Nano Lett. 9(2), 882–886 (2009).
[Crossref] [PubMed]

2008 (7)

A. S. Alkindi, Y. M. Al-Wahaibi, and A. H. Muggeridge, “Physical properties (density, excess molar volume, viscosity, surface tension, and refractive index) of ethanol + glycerol,” J. Chem. Eng. Data 53(12), 2793–2796 (2008).
[Crossref]

P. K. Jain, X. Huang, I. H. El-Sayed, and M. A. El-Sayed, “Noble metals on the nanoscale: optical and photothermal properties and some applications in imaging, sensing, biology, and medicine,” Acc. Chem. Res. 41(12), 1578–1586 (2008).
[Crossref] [PubMed]

H. Chen, X. Kou, Z. Yang, W. Ni, and J. Wang, “Shape- and size-dependent refractive index sensitivity of gold nanoparticles,” Langmuir 24(10), 5233–5237 (2008).
[Crossref] [PubMed]

T. Sannomiya, C. Hafner, and J. Voros, “In situ sensing of single binding events by localized surface plasmon resonance,” Nano Lett. 8(10), 3450–3455 (2008).
[Crossref] [PubMed]

K. M. Mayer, S. Lee, H. Liao, B. C. Rostro, A. Fuentes, P. T. Scully, C. L. Nehl, and J. H. Hafner, “A label-free immunoassay based upon localized surface plasmon resonance of gold nanorods,” ACS Nano 2(4), 687–692 (2008).
[Crossref] [PubMed]

J. N. Anker, W. P. Hall, O. Lyandres, N. C. Shah, J. Zhao, and R. P. Van Duyne, “Biosensing with plasmonic nanosensors,” Nat. Mater. 7(6), 442–453 (2008).
[Crossref] [PubMed]

J. Zhao, A. O. Pinchuk, J. M. McMahon, S. Li, L. K. Ausman, A. L. Atkinson, and G. C. Schatz, “Methods for describing the electromagnetic properties of silver and gold nanoparticles,” Acc. Chem. Res. 41(12), 1710–1720 (2008).
[Crossref] [PubMed]

2007 (1)

E. M. Larsson, J. Alegret, M. Käll, and D. S. Sutherland, “Sensing characteristics of NIR localized surface plasmon resonances in gold nanorings for application as ultrasensitive biosensors,” Nano Lett. 7(5), 1256–1263 (2007).
[Crossref] [PubMed]

2006 (2)

C. L. Nehl, H. Liao, and J. H. Hafner, “Optical properties of star-shaped gold nanoparticles,” Nano Lett. 6(4), 683–688 (2006).
[Crossref] [PubMed]

C. Langhammer, Z. Yuan, I. Zorić, and B. Kasemo, “Plasmonic properties of supported Pt and Pd nanostructures,” Nano Lett. 6(4), 833–838 (2006).
[Crossref] [PubMed]

2005 (2)

L. J. Sherry, S.-H. Chang, G. C. Schatz, R. P. Van Duyne, B. J. Wiley, and Y. Xia, “Localized surface plasmon resonance spectroscopy of single silver nanocubes,” Nano Lett. 5(10), 2034–2038 (2005).
[Crossref] [PubMed]

C. Sönnichsen, B. M. Reinhard, J. Liphardt, and A. P. Alivisatos, “A molecular ruler based on plasmon coupling of single gold and silver nanoparticles,” Nat. Biotechnol. 23(6), 741–745 (2005).
[Crossref] [PubMed]

2003 (1)

K. L. Kelly, E. Coronado, L. L. Zhao, and G. C. Schatz, “The optical properties of metal nanoparticles: the influence of size, shape, and dielectric environment,” J. Phys. Chem. B 107(3), 668–677 (2003).
[Crossref]

2002 (1)

A. J. Haes and R. P. Van Duyne, “A Nanoscale Optical Biosensor: Sensitivity and selectivity of an approach based on the localized surface plasmon resonance spectroscopy of triangular silver nanoparticles,” J. Am. Chem. Soc. 124(35), 10596–10604 (2002).
[Crossref] [PubMed]

1994 (1)

S. Underwood and P. Mulvaney, “Effect of the solution refractive index on the color of gold colloids,” Langmuir 10(10), 3427–3430 (1994).
[Crossref]

1993 (2)

J. Tiggesbaeumker, L. Koeller, K. H. Meiwes-Broer, and A. Liebsch, “Blue shift of the Mie plasma frequency in silver clusters and particles,” Phys. Rev. A: At. Mol. Opt. Phys. 48(3), R1749–R1752 (1993).
[Crossref]

S. Fedrigo, W. Harbich, and J. Buttet, “Collective dipole oscillations in small silver clusters embedded in rare-gas matrices,” Phys. Rev. B Condens. Matter Mater. Phys. 47(16), 10706–10715 (1993).
[Crossref]

Adams, S. M.

S. Campione, S. M. Adams, R. Ragan, and F. Capolino, “Comparison of electric field enhancements: linear and triangular oligomers versus hexagonal arrays of plasmonic nanospheres,” Opt. Express 21(7), 7957–7973 (2013).
[Crossref] [PubMed]

S. M. Adams, S. Campione, J. D. Caldwell, F. J. Bezares, J. C. Culbertson, F. Capolino, and R. Ragan, “Non-lithographic SERS substrates: tailoring surface chemistry for Au nanoparticle cluster assembly,” Small 8(14), 2239–2249 (2012).
[Crossref] [PubMed]

Aherne, D.

D. E. Charles, D. Aherne, M. Gara, D. M. Ledwith, Y. K. Gun’ko, J. M. Kelly, W. J. Blau, and M. E. Brennan-Fournet, “Versatile solution phase triangular silver nanoplates for highly sensitive plasmon resonance sensing,” ACS Nano 4(1), 55–64 (2010).
[Crossref] [PubMed]

Akselrod, G. M.

G. M. Akselrod, C. Argyropoulos, T. B. Hoang, C. Ciracì, C. Fang, J. Huang, D. R. Smith, and M. H. Mikkelsen, “Probing the mechanisms of large Purcell enhancement in plasmonic nanoantennas,” Nat. Photonics 8(11), 835–840 (2014).
[Crossref]

Alegret, J.

E. M. Larsson, J. Alegret, M. Käll, and D. S. Sutherland, “Sensing characteristics of NIR localized surface plasmon resonances in gold nanorings for application as ultrasensitive biosensors,” Nano Lett. 7(5), 1256–1263 (2007).
[Crossref] [PubMed]

Alivisatos, A. P.

C. Sönnichsen, B. M. Reinhard, J. Liphardt, and A. P. Alivisatos, “A molecular ruler based on plasmon coupling of single gold and silver nanoparticles,” Nat. Biotechnol. 23(6), 741–745 (2005).
[Crossref] [PubMed]

Alkindi, A. S.

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S. Fedrigo, W. Harbich, and J. Buttet, “Collective dipole oscillations in small silver clusters embedded in rare-gas matrices,” Phys. Rev. B Condens. Matter Mater. Phys. 47(16), 10706–10715 (1993).
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D. E. Charles, D. Aherne, M. Gara, D. M. Ledwith, Y. K. Gun’ko, J. M. Kelly, W. J. Blau, and M. E. Brennan-Fournet, “Versatile solution phase triangular silver nanoplates for highly sensitive plasmon resonance sensing,” ACS Nano 4(1), 55–64 (2010).
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M. Thämer, A. Kartouzian, P. Heister, T. Lünskens, S. Gerlach, and U. Heiz, “Small supported plasmonic silver clusters,” Small 10(12), 2340–2344 (2014).
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J. N. Anker, W. P. Hall, O. Lyandres, N. C. Shah, J. Zhao, and R. P. Van Duyne, “Biosensing with plasmonic nanosensors,” Nat. Mater. 7(6), 442–453 (2008).
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S. Fedrigo, W. Harbich, and J. Buttet, “Collective dipole oscillations in small silver clusters embedded in rare-gas matrices,” Phys. Rev. B Condens. Matter Mater. Phys. 47(16), 10706–10715 (1993).
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M. J. Banholzer, N. Harris, J. E. Millstone, G. C. Schatz, and C. A. Mirkin, “abnormally large plasmonic shifts in silica-protected gold triangular nanoprisms,” J. Phys. Chem. C 114(16), 7521–7526 (2010).
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M. Thämer, A. Kartouzian, P. Heister, T. Lünskens, S. Gerlach, and U. Heiz, “Small supported plasmonic silver clusters,” Small 10(12), 2340–2344 (2014).
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T. Lünskens, P. Heister, M. Thämer, C. A. Walenta, A. Kartouzian, and U. Heiz, “Plasmons in supported size-selected silver nanoclusters,” Phys. Chem. Chem. Phys. 17(27), 17541–17544 (2015).
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M. Thämer, A. Kartouzian, P. Heister, T. Lünskens, S. Gerlach, and U. Heiz, “Small supported plasmonic silver clusters,” Small 10(12), 2340–2344 (2014).
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G. M. Akselrod, C. Argyropoulos, T. B. Hoang, C. Ciracì, C. Fang, J. Huang, D. R. Smith, and M. H. Mikkelsen, “Probing the mechanisms of large Purcell enhancement in plasmonic nanoantennas,” Nat. Photonics 8(11), 835–840 (2014).
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X. Huang, S. Tang, X. Mu, Y. Dai, G. Chen, Z. Zhou, F. Ruan, Z. Yang, and N. Zheng, “Freestanding palladium nanosheets with plasmonic and catalytic properties,” Nat. Nanotechnol. 6(1), 28–32 (2011).
[Crossref] [PubMed]

P. K. Jain, X. Huang, I. H. El-Sayed, and M. A. El-Sayed, “Noble metals on the nanoscale: optical and photothermal properties and some applications in imaging, sensing, biology, and medicine,” Acc. Chem. Res. 41(12), 1578–1586 (2008).
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Y.-F. Chang, S.-H. Hung, Y.-J. Lee, R.-C. Chen, L.-C. Su, C.-S. Lai, and C. Chou, “Discrimination of breast cancer by measuring prostate-specific antigen levels in women’s serum,” Anal. Chem. 83(13), 5324–5328 (2011).
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J. McPhillips, A. Murphy, M. P. Jonsson, W. R. Hendren, R. Atkinson, F. Höök, A. V. Zayats, and R. J. Pollard, “High-performance biosensing using arrays of plasmonic nanotubes,” ACS Nano 4(4), 2210–2216 (2010).
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T. Pakizeh, C. Langhammer, I. Zorić, P. Apell, and M. Käll, “Intrinsic Fano Interference of Localized Plasmons in Pd Nanoparticles,” Nano Lett. 9(2), 882–886 (2009).
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[Crossref] [PubMed]

M. Thämer, A. Kartouzian, P. Heister, T. Lünskens, S. Gerlach, and U. Heiz, “Small supported plasmonic silver clusters,” Small 10(12), 2340–2344 (2014).
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D. E. Charles, D. Aherne, M. Gara, D. M. Ledwith, Y. K. Gun’ko, J. M. Kelly, W. J. Blau, and M. E. Brennan-Fournet, “Versatile solution phase triangular silver nanoplates for highly sensitive plasmon resonance sensing,” ACS Nano 4(1), 55–64 (2010).
[Crossref] [PubMed]

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K. L. Kelly, E. Coronado, L. L. Zhao, and G. C. Schatz, “The optical properties of metal nanoparticles: the influence of size, shape, and dielectric environment,” J. Phys. Chem. B 107(3), 668–677 (2003).
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T. A. F. König, P. A. Ledin, J. Kerszulis, M. A. Mahmoud, M. A. El-Sayed, J. R. Reynolds, and V. V. Tsukruk, “Electrically tunable plasmonic behavior of nanocube-polymer nanomaterials induced by a redox-active electrochromic polymer,” ACS Nano 8(6), 6182–6192 (2014).
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Y. Khalavka, J. Becker, and C. Sönnichsen, “Synthesis of rod-shaped gold nanorattles with improved plasmon sensitivity and catalytic activity,” J. Am. Chem. Soc. 131(5), 1871–1875 (2009).
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L. Tian, J. J. Morrissey, R. Kattumenu, N. Gandra, E. D. Kharasch, and S. Singamaneni, “Bioplasmonic paper as a platform for detection of kidney cancer biomarkers,” Anal. Chem. 84(22), 9928–9934 (2012).
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H. Chen, X. Kou, Z. Yang, W. Ni, and J. Wang, “Shape- and size-dependent refractive index sensitivity of gold nanoparticles,” Langmuir 24(10), 5233–5237 (2008).
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Y. Yang, I. I. Kravchenko, D. P. Briggs, and J. Valentine, “All-dielectric metasurface analogue of electromagnetically induced transparency,” Nat. Commun. 5, 5753 (2014).
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Y.-F. Chang, S.-H. Hung, Y.-J. Lee, R.-C. Chen, L.-C. Su, C.-S. Lai, and C. Chou, “Discrimination of breast cancer by measuring prostate-specific antigen levels in women’s serum,” Anal. Chem. 83(13), 5324–5328 (2011).
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T. Pakizeh, C. Langhammer, I. Zorić, P. Apell, and M. Käll, “Intrinsic Fano Interference of Localized Plasmons in Pd Nanoparticles,” Nano Lett. 9(2), 882–886 (2009).
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J. N. Anker, W. P. Hall, O. Lyandres, N. C. Shah, J. Zhao, and R. P. Van Duyne, “Biosensing with plasmonic nanosensors,” Nat. Mater. 7(6), 442–453 (2008).
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L. Tian, J. J. Morrissey, R. Kattumenu, N. Gandra, E. D. Kharasch, and S. Singamaneni, “Bioplasmonic paper as a platform for detection of kidney cancer biomarkers,” Anal. Chem. 84(22), 9928–9934 (2012).
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G. M. Akselrod, C. Argyropoulos, T. B. Hoang, C. Ciracì, C. Fang, J. Huang, D. R. Smith, and M. H. Mikkelsen, “Probing the mechanisms of large Purcell enhancement in plasmonic nanoantennas,” Nat. Photonics 8(11), 835–840 (2014).
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J. J. Mock, S. M. Norton, S.-Y. Chen, A. A. Lazarides, and D. R. Smith, “Electromagnetic Enhancement Effect Caused by Aggregation on SERS-Active Gold Nanoparticles,” Plasmonics 6(1), 113–124 (2011).
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T. A. F. König, P. A. Ledin, J. Kerszulis, M. A. Mahmoud, M. A. El-Sayed, J. R. Reynolds, and V. V. Tsukruk, “Electrically tunable plasmonic behavior of nanocube-polymer nanomaterials induced by a redox-active electrochromic polymer,” ACS Nano 8(6), 6182–6192 (2014).
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N. Omura, I. Uechi, and S. Yamada, “Comparison of plasmonic sensing between polymer- and silica-coated gold nanorods,” Anal. Sci. 25(2), 255–259 (2009).
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L. J. Sherry, S.-H. Chang, G. C. Schatz, R. P. Van Duyne, B. J. Wiley, and Y. Xia, “Localized surface plasmon resonance spectroscopy of single silver nanocubes,” Nano Lett. 5(10), 2034–2038 (2005).
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Y. H. Lee, H. Chen, Q.-H. Xu, and J. Wang, “Refractive index sensitivities of noble metal nanocrystals: the effects of multipolar plasmon resonances and the metal type,” J. Phys. Chem. C 115(16), 7997–8004 (2011).
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K. Sugawa, H. Tahara, A. Yamashita, J. Otsuki, T. Sagara, T. Harumoto, and S. Yanagida, “Refractive index susceptibility of the plasmonic palladium nanoparticle: potential as the third plasmonic sensing material,” ACS Nano 9(2), 1895–1904 (2015).
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Figures (5)

Fig. 1
Fig. 1 Pd nanoplates synthesized in this study. (a)-(c) BF-STEM and (d) HAADF-STEM images and (e) Schematic illustration and model structure approximated by a regular polygon with 40 sides. E and k are the electric field vector and the wave vector of the inciendent light.
Fig. 2
Fig. 2 Extinction spectrum of the Pd nanoplates. (a) Observed spectrum for a colloidal ethanol solution. (b) Calculated spectrum (RI of the surrounding medium: 1.361) of the Pd nanoplate (Fig. 1(e)).
Fig. 3
Fig. 3 Shifts of extinction peak of the Pd nanoplates dispersed in media with different RI. Spectra are normalized to highlight the spectral shift. (a) Observed extinction spectra of the Pd nanoplates dispersed in different solvent mixtures (10, 20, 30, 40, and 50 vol. % glycerol ethanol solutions). (b) Calculated extinction spectra of the Pd nanoplates in different RI solvents (n = 1.375, 1.388, 1.401, 1.413, and 1.425 corresponding to ethanol containing 10, 20, 30, 40, and 50 vol.% glycerol, respectively). (c) Dependences of the LSPR peak shifts upon RI changes from (A) experimental and (B) theoretical results.
Fig. 4
Fig. 4 (a) Schematic illustration of PVP-coated Pd nanoplate. (b) Theoretical dependences of the LSPR peak shifts upon RI changes of (A) the bare Pd nanoplate (same as (B) in Fig. 3(c)) and (B) the PVP-coated Pd nanoplate and experimental dependence of the peak shifts of (C) the nanoplates (same as (A) in Fig. 3(c)).
Fig. 5
Fig. 5 (a) Theoretical dependences of the LSPR peak shifts upon RI changes of the Pd nanoplates with the PVP of (A) 0, (B) 0.6, (C) 0.9, (D) 1.2, (E) 1.8, and (F) 2.4 nm in thicknesses. (b) PVP thickness dependence of the RI susceptibility of the Pd nanoplates.

Equations (1)

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n( mixed  solvent )=0.0104 ( 0.0171a 0.0171a+0.0137b ) 3 0.0362 ( 0.0171a 0.0171a+0.0137b ) 2                                0.0658( 0.0171a 0.0171a+0.0137b )+1.4742

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